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Beilstein J. Org. Chem. 2011, 7, 1164–1172, doi:10.3762/bjoc.7.135
Graphical Abstract
Scheme 1: Eschenmoser coupling reaction with secondary S-alkylated thioamide derivatives of type 3.
Scheme 2: Eschenmoser coupling sequence of S-alkylated ternary thioamides of type 7.
Figure 1: Conversion of 3aa to 4aa under different flow conditions.
Figure 2: Reaction kinetics analysis. Left: Rate constants with 0.1 M reaction solution. Right: Arrhenius-plo...
Scheme 3: Exclusive formation of thiazol 13 with dihydropyrimidine derivatives 11 take place in the case of a...
Figure 3: Flow chemistry setup scheme.
Figure 4: Capillary reactor with jacketed cover removed, and the process controller.